--- title: "Introduction to fluxfinder" output: rmarkdown::html_vignette vignette: > %\VignetteIndexEntry{Introduction to fluxfinder} %\VignetteEngine{knitr::rmarkdown} %\VignetteEncoding{UTF-8} --- ```{r, include = FALSE} knitr::opts_chunk$set( collapse = TRUE, comment = "#>" ) ``` The `fluxfinder` package provides functions to parse static-chamber greenhouse gas measurement files generated by a variety of instruments; compute flux rates using multi-observation metadata; and generate diagnostic metrics and plots. It's designed to be easy to integrate into scientific workflows. ## Load sample data ```{r setup} library(fluxfinder) # Data from a LI-7810 f <- system.file("extdata/TG10-01087.data", package = "fluxfinder") dat <- ffi_read_LI7810(f) # Note that the fluxfinder read functions print some info after reading # Set "options(fluxfinder.quiet = TRUE)" to suppress such messages # Look at a subset of the data; the full data frame has 500+ rows and 25 columns dat[1:6, 1:9] ``` The data frame returned by `ffi_read_LI7810` is all data from the raw [LI-7810](https://www.licor.com/env/products/trace-gas/LI-7810) file, except that `TIMESTAMP`, `TZ` (time zone of the timestamps), `SN` (serial number), and `MODEL` columns have been added. The analyzer data is basically a stream of measured greenhouse gas concentrations: ```{r overview-plot, fig.width=7} library(ggplot2) ggplot(dat, aes(TIMESTAMP, CO2)) + geom_point() ``` ## Match with metadata For these data to be useful, we need to associate them with _metadata_ about the measurements: when they were started, how long they lasted, plot/treatment/collar information, etc. ```{r metadata} # Accompanying metadata md <- system.file("extdata/TG10-01087-metadata.csv", package = "fluxfinder") metadat <- read.csv(md) print(metadat) ``` **Important note**: in this sample metadata, our measurement identified is labeled `Plot`, but this could be named, and refer to, anything: bottle, sample, collar, etc. It's simply an identifier for _this_ measurement, i.e. this row. The `ffi_metadata_match` function matches up the data with metadata, using the `TIMESTAMP` column that `ffi_read_LI7810` helpfully created when it read the data file. ```{r matching, fig.width=7} dat$metadat_row <- ffi_metadata_match( data_timestamps = dat$TIMESTAMP, start_dates = metadat$Date, start_times = metadat$Start_time, obs_lengths = metadat$Obs_length + 10) # 10 is expected dead band length # Note that ffi_metadata_match() warns us that one metadata row didn't match any data # Based on the row match information, add a "Plot" column to the data dat$Plot <- metadat$Plot[dat$metadat_row] metadat$metadat_row <- seq_len(nrow(metadat)) # ...and plot p <- ggplot(dat, aes(TIMESTAMP, CO2, color = Plot)) + geom_point() print(p) ``` Some of these are clearly not correct--the measurement time seems to be shorter then 60 seconds for the C, D, and E plots: ```{r emphasize-problems, fig.width=7, echo=FALSE, message=FALSE} library(lubridate) p + annotate("rect", ymin = 455, ymax = 476, xmin = ymd_hms("2022-10-27 10:39:30", tz = "EST"), xmax = ymd_hms("2022-10-27 10:43:30", tz = "EST"), color = "red", fill = NA, linewidth = 1.5) ``` In real life we'd want to correct the faulty metadata at its source. Here, we'll just change the values programmatically and re-match: ```{r matching2, fig.width=7} metadat$Obs_length[3:5] <- c(30, 45, 45) dat$metadat_row <- ffi_metadata_match( data_timestamps = dat$TIMESTAMP, start_dates = metadat$Date, start_times = metadat$Start_time, obs_lengths = metadat$Obs_length + 10) dat$Plot <- metadat$Plot[dat$metadat_row] p %+% dat ``` That looks better! ## Unit conversion We'd like our final units to be in µmol/m2/s, and so need to do some unit conversion. (This can happen either before or after flux computation, below.) The package provides `ffi_ppm_to_umol()` and `ffi_ppb_to_nmol()` functions that perform this conversion using the [Ideal Gas Law](https://en.wikipedia.org/wiki/Ideal_gas_law). ```{r units} dat$CO2_umol <- ffi_ppm_to_umol(dat$CO2, volume = 0.1, # m3 temp = 24) # degrees C # See the message: because we didn't provide the 'atm' parameter, # ffi_ppm_to_umol assumed standard pressure. # Also normalize by ground area (0.16 m2 in this example) dat$CO2_umol_m2 <- dat$CO2_umol / 0.16 ``` Note that in the example above we're using a **constant system volume and measurement ground area**. If that's not the case, there should be a column in the metadata providing the changing values (e.g. giving volume in m3) for each measurement. Then after calling `ffi_metadata_match()`, merge the data and metadata and pass the appropriate column to `ffi_ppm_to_umol()`. Here's an example: ```{r} # Let's say volume varies by measurement; this can happen if the chamber # height changes depending on the ground vegetation in each plot metadat$Volume <- c(0.1, 0.2, 0.1, 0.1, 0.3, 0.1, 0.1) # Merge the data and metadata dat_changing_vol <- merge(dat, metadat[c("Plot", "Volume")], by = "Plot", all.x = TRUE) # Unit conversion as above, but using the changing volume information: dat_changing_vol$CO2_umol <- ffi_ppm_to_umol(dat_changing_vol$CO2, volume = dat_changing_vol$Volume, temp = 24) # We still have constant ground area in this example dat_changing_vol$CO2_umol_m2 <- dat_changing_vol$CO2_umol / 0.16 # Relative to the previous constant-volume example, our area-normalized # amounts (µmol) have now increased for plots B and E because # of their larger volumes: aggregate(CO2_umol_m2 ~ Plot, data = dat, FUN = mean) aggregate(CO2_umol_m2 ~ Plot, data = dat_changing_vol, FUN = mean) ``` ## Compute fluxes The `ffi_compute_fluxes` function provides a general-purpose tool for computing fluxes from concentration time series, as well as associated QA/QC information. It returns statistics for four types of models: _linear_, _robust linear_, _polynomial_, and _HM81_, an exponential model derived from diffusion theory, following [Hutchinson and Mosier (1981)](http://dx.doi.org/10.2136/sssaj1981.03615995004500020017x). Model statistics include Akaike information criterion (`AIC`), R squared (`r.squared`), standard error of the residuals (`sigma`), and model p-value (`p.value`). For the robust linear regression only, a logical value `converged` is included; see the documentation for `MASS::rlm()`. Flux (slope) statistics estimate and std.error; For the robust linear regression model only, a logical value converged. ```{r compute-fluxes} fluxes <- ffi_compute_fluxes(dat, group_column = "Plot", time_column = "TIMESTAMP", gas_column = "CO2_umol_m2", dead_band = 10) # By default, ffi_compute_fluxes returns a data.frame with one row per # grouping variable value (i.e., per measurement). The first column is the # group label; the second is the average value of the `time_column`; # and the rest of the columns are fit statistics for a linear fit of # concentration as a function of time, along with information about polynomial # and robust-linear fits. See ?ffi_compute_fluxes for more details. names(fluxes) # For clarity, print out only a subset of the columns fluxes[c("Plot", "TIMESTAMP", "lin_r.squared", "lin_flux.estimate", "HM81_flux.estimate")] ``` Note that the `fluxes` extract printed above has one row per `Plot`, the grouping variable; the mean `TIMESTAMP` of the group; model statistics such as `lin_r.squared`; and the flux estimate. The final column, `HM81_flux.estimate` is only numeric (i.e., not `NA`) when the data show evidence of a saturating curvature. So in this case we might want to examine more carefully the data from plots A, C, and F. Plotting our computed fluxes: ```{r plot-fluxes, fig.width=7} ggplot(fluxes, aes(Plot, lin_flux.estimate, color = lin_r.squared)) + geom_point() + geom_linerange(aes(ymin = lin_flux.estimate - lin_flux.std.error, ymax = lin_flux.estimate + lin_flux.std.error)) + ylab("CO2 flux (µmol/m2/s)") ``` We might want to check whether the robust-linear slope diverges from the linear fit slope, suggesting influential outliers, or whether the polynomial R2 is much larger, potentially indicating curvature of the observations due to e.g. diffusion limitations. ```{r, figures-side, fig.show="hold", out.width="46%"} ggplot(fluxes, aes(lin_flux.estimate, rob_flux.estimate, color = Plot)) + geom_point() + geom_abline() + theme(legend.position = "none") ggplot(fluxes, aes(lin_r.squared, poly_r.squared, color = Plot)) + geom_point() + geom_abline() + theme(legend.position="none") ``` The plot C (green) data have more scatter, and thus lower R2 values and higher uncertainty on the computed flux, but there's no strong evidence of nonlinearity or outlier problems (although see note above about the `HM81_estimate` field). ## A clearly nonlinear case In our experience, static-chamber fluxes are frequently linear ([Forbrich et al. 2010](https://doi.org/10.1016/j.soilbio.2009.12.004)) even though molecular diffusion means that chamber feedbacks will inevitably lead to curvilinear (saturating) behavior over time ([Pedersen et al. 2010](https://doi.org/10.1111/j.1365-2389.2010.01291.x)). Still, how does one use `fluxfinder` to diagnose and work with nonlinear data? Let's use R's built-in `Puromycin` dataset (simply because it exhibits saturating behavior; it's unrelated to greenhouse gases) as an example: ```{r, fig.width=7} ggplot(Puromycin, aes(conc, rate)) + geom_point() + geom_smooth(method = "lm") ``` Visually, we can see that a linear model will not be appropriate in this case. ```{r} ffi_compute_fluxes(Puromycin, group_column = NULL, time_column = "conc", gas_column = "rate") ``` ```{r include=FALSE} x <- ffi_compute_fluxes(Puromycin, group_column = NULL, time_column = "conc", gas_column = "rate") x <- round(x, 3) ``` From the diagnostics returned by `ffi_compute_fluxes`: * `HM81_flux.estimate` is not `NA`, which only occurs with saturating behavior; * The `lin_AIC` (`r x$lin_AIC`) and `rob_AIC` (`r x$rob_AIC`) [Akaike information criterion](https://en.wikipedia.org/wiki/Akaike_information_criterion) values are similar, so no indication of influential outliers; * The `lin_r.squared` (`r x$lin_r.squared`) and `poly_r.squared` (`r x$poly_r.squared`) values are _very_ different, suggesting a failure of the linear model; * The [root mean square error](https://en.wikipedia.org/wiki/Root_mean_square_deviation) (RMSE) of the linear model is much higher than the other models' values; * The `HM81_r.squared` (`r x$HM81_r.squared`) and `HM81_AIC` (`r x$HM81_AIC`) are considerably higher and lower, respectively, than the linear model. All of these metrics point to a common conclusion: a linear model is _not_ appropriate for these data. If these were real data, we should use the `HM81_flux.estimate` value as our flux estimate. ## Conclusion This vignette covered `fluxfinder` basics: loading data and metadata, matching the two, performing unit conversion, computing fluxes, and some basic QA/QC. The test data we worked above could be fit well by linear model, but for many reasons this might not always be true; see the vignette on [integrating with the gasfluxes package](integrating-gasfluxes.html) for guidance on using more sophisticated model-fitting routines.